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农学学报 ›› 2017, Vol. 7 ›› Issue (11): 51-61.doi: 10.11923/j.issn.2095-4050.cjas17040017

• 农业工程 农业机械 生物技术 食品科学 • 上一篇    下一篇

白胡椒加工过程中的风味物质分析

吴桂苹,谷风林,房一明,朱红英   

  1. 中国热带农业科学院香料饮料研究所,中国热带农业科学院香料饮料研究所,中国热带农业科学院香料饮料研究所,中国热带农业科学院香料饮料研究所
  • 收稿日期:2017-04-14 修回日期:2017-05-22 接受日期:2017-06-08 出版日期:2017-11-28 发布日期:2017-11-28
  • 通讯作者: 谷风林 E-mail:9mjnm7
  • 基金资助:
    海南省自然科学基金面上项目“白胡椒加工中微生物菌群分析研究”(20163135);中国热带农业科学院基本科研业务费专项资金“天然香 辛饮料纳米微胶囊制备研究”(1630142017020)。

Analysis of Flavour Compounds of White Pepper During Processing

  • Received:2017-04-14 Revised:2017-05-22 Accepted:2017-06-08 Online:2017-11-28 Published:2017-11-28

摘要: 为研究白胡椒加工过程中风味物质的变化,探讨异味物质的形成,以胡椒鲜果为原料,静水和换水浸泡2 种方式加工白胡椒,采用顶空固相微萃取和水蒸气蒸馏法萃取白胡椒粒风味物质,气相色谱-质谱联用仪检测分析浸泡3 天、6 天以及终极产品中风味物质组成及差异。白胡椒粒中共检测出167 种化合物,β-石竹烯相对含量最高,达到总组分的20.64%~28.31%,其次是柠檬烯,相对含量为6.89%~11.24%。在静水浸泡的白胡椒中检测到异臭物质3-甲基吲哚。白胡椒精油中共检测出31 种化合物,3-蒈烯(21.94%~24.64%)、β-石竹烯(17.51%~22.21%)、柠檬烯(18.04%~19.26%)、β-蒎烯(9.63%~10.67%)、α-蒎烯(4.46%~5.65%)、水芹烯(6.70%~7.53%)和月桂烯(3.44%~3.84%)等萜类化合物是白胡椒的主要风味物质。胡椒鲜果静水浸泡3天即能产生异臭味,而采用换水加工的白胡椒未检出异臭物质。

关键词: 生物质炭, 生物质炭, 漂浮育苗, 烟苗生长

Abstract: To explore the formation of off-flavour compounds, the ?avour components of white pepper were analyzed at different processing steps. Using the fresh pepper fruit as raw material, the static and exchanging water soaking methods were used for processing white pepper. The flavour compounds were extracted by headspace solid phase micro-extraction and steam distillation, and identified by gas chromatography-mass spectrometry (GC-MS). The flavour composition and differences were analyzed for the samples of soaking 3 days, 6 days and the final products. The results showed that 167 compounds were detected in white pepper corn and the content of β-caryophyllene was the highest, ranging from 20.64% to 28.31% of relative content. Secondly, limonene content was between 6.89% and 11.24%.The off-flavour compound (3-methyl indole) was detected in white pepper prepared by soaking in static water. A total of 31 compounds were detected in white pepper essential oil, in which terpenoids such as 3-carene (21.94%-24.64%), β-caryophyllene (17.51%-22.21%), limonene (18.04%-19.26%), β-pinene (9.63%-10.67%) were the major flavour components of white pepper. The off-flavour could be detected in static water soaking for 3 days, but the off-flavour were not found in the white pepper prepared from exchanging water.

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